6CAS
Serial Femtosecond X-ray Crystal Structure of 30S ribosomal subunit from Thermus thermophilus in complex with N1MS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.98 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 402.100, 402.100, 175.100 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.190 - 3.500 |
R-factor | 0.2475 |
Rwork | 0.247 |
R-free | 0.27730 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.647 |
Data reduction software | MOSFLM |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.190 | 39.190 |
High resolution limit [Å] | 3.500 | 3.500 |
Number of reflections | 175871 | |
<I/σ(I)> | 2.29 | |
Completeness [%] | 100.0 | |
Redundancy | 131 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 6.5 | 298 | 17% MPD |