6C5D
N-terminal domain of Helicobacter pylori LlaJI.R1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-21 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9791 |
Spacegroup name | P 1 |
Unit cell lengths | 37.526, 43.771, 85.091 |
Unit cell angles | 97.87, 93.86, 97.77 |
Refinement procedure
Resolution | 83.970 - 1.970 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 83.970 | 2.100 |
High resolution limit [Å] | 1.970 | 1.970 |
Rmeas | 0.096 | 0.624 |
Number of reflections | 152937 | 23180 |
<I/σ(I)> | 9 | 1.56 |
Completeness [%] | 93.6 | 90.1 |
Redundancy | 3.68 | 1.91 |
CC(1/2) | 0.997 | 0.709 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 298 | 0.1 M MMT, pH 6.5, 25% v/v PEG1500 |