Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.3.1 |
| Synchrotron site | ALS |
| Beamline | 8.3.1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-05-31 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 1.11583 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 161.166, 160.159, 198.502 |
| Unit cell angles | 90.00, 109.97, 90.00 |
Refinement procedure
| Resolution | 151.474 - 2.503 |
| R-factor | 0.2003 |
| Rwork | 0.198 |
| R-free | 0.24620 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.837 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | MOLREP |
| Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 152.000 | 2.660 |
| High resolution limit [Å] | 2.500 | 2.500 |
| Number of reflections | 632259 | |
| <I/σ(I)> | 7.99 | |
| Completeness [%] | 98.2 | |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 298 | 45% MPD, 0.2 M Na formate |
