6C4L
Yersinopine dehydrogenase (YpODH) - Apo
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-05-06 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9794 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 97.902, 124.125, 87.981 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.890 - 2.000 |
R-factor | 0.2021 |
Rwork | 0.200 |
R-free | 0.24530 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.008 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | CRANK2 |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.430 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.082 | 1.039 |
Number of reflections | 36673 | 2550 |
<I/σ(I)> | 8.7 | |
Completeness [%] | 99.6 | |
Redundancy | 6.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 3.5 M sodium formation pH 6 |