6C3Z
T477A SiRHP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-10-17 |
Detector | MARRESEARCH |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 68.223, 77.317, 87.277 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.658 - 1.681 |
R-factor | 0.1963 |
Rwork | 0.194 |
R-free | 0.24680 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1aop |
RMSD bond length | 0.008 |
RMSD bond angle | 1.260 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.658 | 2.000 |
High resolution limit [Å] | 1.681 | 1.900 |
Number of reflections | 39731 | 2597 |
<I/σ(I)> | 13.2 | |
Completeness [%] | 95.8 | 73 |
Redundancy | 11.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 7.8 | 273 | 65 mM potassium phosphate, 20% PEG 8000, 1 mM EDTA |