6C3Y

Wild type structure of SiRHP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 22-ID
Synchrotron site	APS
Beamline	22-ID
Temperature [K]	100
Detector technology	CCD
Collection date	2017-10-17
Detector	MARRESEARCH
Wavelength(s)	1.0
Spacegroup name	P 21 21 21
Unit cell lengths	67.823, 77.262, 87.614
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.600 - 1.542
R-factor	0.1654
Rwork	0.165
R-free	0.19470
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1aop
RMSD bond length	0.008
RMSD bond angle	1.450
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.11.1_2575: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	38.600	1.600
High resolution limit [Å]	1.500	1.500
Number of reflections	67052	5732
<I/σ(I)>	13.9
Completeness [%]	97.8	84.2
Redundancy	10.6	2.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION	7.8	273	65 mM potassium phosphate, 20% PEG 8000, 1 mM EDTA