6C3M
Wild type structure of SiRHP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-10-17 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 68.398, 77.223, 87.214 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.600 - 1.500 |
R-factor | 0.1668 |
Rwork | 0.166 |
R-free | 0.18590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1aop |
RMSD bond length | 0.008 |
RMSD bond angle | 1.531 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.000 | 1.600 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 68383 | 6514 |
<I/σ(I)> | 15.2 | |
Completeness [%] | 99.4 | 95.8 |
Redundancy | 9.7 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 7.8 | 293 | 65 mM Potassium Phosphate 18% PEG 8000 1 mM EDTA |