6C10
Crystal structure of mouse PCDH15 EC11-EL
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-18 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.98 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 57.680, 57.680, 159.180 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.230 - 1.399 |
R-factor | 0.1706 |
Rwork | 0.169 |
R-free | 0.19510 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.733 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | Auto-Rickshaw |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.230 | 1.450 |
High resolution limit [Å] | 1.400 | 1.400 |
Number of reflections | 53914 | |
<I/σ(I)> | 25.05 | |
Completeness [%] | 99.7 | |
Redundancy | 9.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 0.2 M Lithium sulfate, 30% (w/v) PEG4000, 0.1 M Tris pH 8.5 |