6BXF

Crystal structure of an extended b3 integrin L33

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-F
Synchrotron site	APS
Beamline	21-ID-F
Temperature [K]	100
Detector technology	CCD
Collection date	2016-07-23
Detector	MAR CCD 130 mm
Wavelength(s)	0.97872
Spacegroup name	P 1 21 1
Unit cell lengths	59.070, 81.470, 127.960
Unit cell angles	90.00, 97.07, 90.00

Refinement procedure

Resolution	63.490 - 3.200
R-factor	0.2681
Rwork	0.265
R-free	0.33480
RMSD bond length	0.003
RMSD bond angle	0.625
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX ((1.12_2829: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	63.490	3.370
High resolution limit [Å]	3.200	3.200
Number of reflections	20112
<I/σ(I)>	6.5
Completeness [%]	100.0
Redundancy	7.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277	12% PEG 8000, 0.2 M NaCl, 0.1 M HEPES (pH 7.5)