6BPV
Crystal structure of cysteine-bound ferrous form of the matured F2-Tyr157 human cysteine dioxygenase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-04-19 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97622 |
Spacegroup name | P 65 |
Unit cell lengths | 131.435, 131.435, 34.177 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 31.570 - 1.950 |
R-factor | 0.1619 |
Rwork | 0.160 |
R-free | 0.17920 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ic1 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.000 |
High resolution limit [Å] | 1.950 | 4.810 | 1.950 |
Rmerge | 0.163 | 0.116 | 0.768 |
Rmeas | 0.173 | 0.122 | 0.828 |
Rpim | 0.055 | 0.039 | 0.305 |
Number of reflections | 25083 | 1773 | 1659 |
<I/σ(I)> | 4.8 | ||
Completeness [%] | 99.9 | 99.7 | 98.9 |
Redundancy | 9.4 | 9.8 | 6.8 |
CC(1/2) | 0.982 | 0.818 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 295 | 0.1 M MES, 2 M ammonium sulfate, 2% PEG400 |