6BPH
Crystal structure of the chromodomain of RBBP1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-03-18 |
Detector | RIGAKU SATURN A200 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 41.493, 41.493, 81.349 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.900 - 1.850 |
R-factor | 0.207 |
Rwork | 0.206 |
R-free | 0.22600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2lcc |
RMSD bond length | 0.010 |
RMSD bond angle | 0.950 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.32) |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.2) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 36.970 | 36.970 | 1.840 |
High resolution limit [Å] | 1.800 | 9.000 | 1.800 |
Rmerge | 0.072 | 0.026 | 1.077 |
Rmeas | 0.075 | 0.027 | 1.119 |
Rpim | 0.020 | 0.009 | 0.300 |
Total number of observations | 92703 | 728 | 5174 |
Number of reflections | 7057 | ||
<I/σ(I)> | 26.2 | 69.7 | 3.3 |
Completeness [%] | 99.6 | 99.8 | 98.8 |
Redundancy | 13.1 | 8.7 | 13.3 |
CC(1/2) | 1.000 | 1.000 | 0.919 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 25% PEG 3350, 0.2M magnesium chloride, 0.1M HEPES, pH 7.5 |