6BK3
Crystal structure of Os79 from O. sativa in complex with UDP and deoxynivalenol-3-glucoside (glucose moitey not resolved)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-BM |
Synchrotron site | APS |
Beamline | 19-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-08-09 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 0.979 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 104.504, 104.504, 98.261 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.140 - 2.170 |
R-factor | 0.19051 |
Rwork | 0.189 |
R-free | 0.22792 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5tme |
RMSD bond length | 0.022 |
RMSD bond angle | 2.221 |
Data scaling software | HKL-3000 |
Phasing software | FFT |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.170 |
Rmerge | 0.086 |
Number of reflections | 33082 |
<I/σ(I)> | 29.1 |
Completeness [%] | 100.0 |
Redundancy | 11.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 277 | 100 mM sodium acetate pH 5.0, 40% pentaerythritol propoxylate 426, 320 mM NaCl |