6BK0
Crystal structure of Os79 Q202A from O. sativa in complex with UDP.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-15 |
Detector | DECTRIS PILATUS3 X 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.409, 83.233, 99.098 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.460 - 1.470 |
R-factor | 0.15408 |
Rwork | 0.153 |
R-free | 0.18068 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5tme |
RMSD bond length | 0.041 |
RMSD bond angle | 2.874 |
Data scaling software | HKL-3000 |
Phasing software | HKL-3000 |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.470 |
Number of reflections | 79234 |
<I/σ(I)> | 41.3 |
Completeness [%] | 99.2 |
Redundancy | 13.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 100 mM 3-(N- Morpholino)propanesulfonic acid pH 7.5, 15% methyl ether polyethylene glycol 5000 (MEPEG 5K), 160 mM potassium glutamate |