6BJN
PICK1 PDZ domain in complex with the class I PDZ binding motif QSAV
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2013-08-13 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.54 |
Spacegroup name | P 32 |
Unit cell lengths | 54.473, 54.473, 78.119 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.180 - 2.430 |
R-factor | 0.1958 |
Rwork | 0.194 |
R-free | 0.22000 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.929 |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.430 |
Number of reflections | 9544 |
<I/σ(I)> | 7.1 |
Completeness [%] | 99.6 |
Redundancy | 4.8 |
CC(1/2) | 0.860 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.1M BisTRIS pH 5.5 and 25% PEG3350 |