6BIQ
Structure of NlpC2 from Trichomonas vaginalis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2016-01-01 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 |
Unit cell lengths | 36.820, 99.030, 102.839 |
Unit cell angles | 115.02, 96.28, 94.28 |
Refinement procedure
Resolution | 35.695 - 2.300 |
R-factor | 0.201 |
Rwork | 0.199 |
R-free | 0.24140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6bim |
RMSD bond length | 0.006 |
RMSD bond angle | 0.803 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.900 | 2.370 |
High resolution limit [Å] | 2.300 | 2.300 |
Rpim | 0.073 | 0.327 |
Number of reflections | 53546 | 4164 |
<I/σ(I)> | 6.9 | 2 |
Completeness [%] | 93.0 | 89.3 |
Redundancy | 2.9 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.2M Ammonium fluoride 20% PEG3350 |