6BIM

Structure of NlpC1 from Trichomonas vaginalis

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	110
Detector technology	IMAGE PLATE
Collection date	2015-01-01
Detector	MAR scanner 345 mm plate
Wavelength(s)	1.5418
Spacegroup name	P 21 2 21
Unit cell lengths	53.120, 70.060, 79.930
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	29.059 - 1.547
R-factor	0.155
Rwork	0.154
R-free	0.17530
Structure solution method	SIR
RMSD bond length	0.003
RMSD bond angle	0.676
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHENIX
Refinement software	PHENIX ((1.10_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	29.240	1.570
High resolution limit [Å]	1.540	1.540
Rpim	0.030	0.112
Number of reflections	83416	1744
<I/σ(I)>	14.1	4.1
Completeness [%]	98.8	81
Redundancy	5.7	5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		291	Morpheus screen A1