6BE0
AvrA delL154 with IP6, CoA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-10-05 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 1 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 62.931, 62.931, 187.566 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.083 - 2.438 |
R-factor | 0.1892 |
Rwork | 0.187 |
R-free | 0.23100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5klp |
RMSD bond length | 0.003 |
RMSD bond angle | 0.649 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.438 |
Number of reflections | 25168 |
<I/σ(I)> | 31.9 |
Completeness [%] | 99.8 |
Redundancy | 10.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 295 | 8.5% PEG8000, 15% ethylene glycol, 100mM MES pH 5.6 - 5.8 |