6B7L

Aeromonas veronii immune modulator A

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.2
Synchrotron site	ALS
Beamline	5.0.2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-07-16
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	1.0
Spacegroup name	P 6 2 2
Unit cell lengths	160.465, 160.465, 66.180
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	41.142 - 2.300
R-factor	0.1756
Rwork	0.172
R-free	0.20400
Structure solution method	SAD
RMSD bond length	0.008
RMSD bond angle	1.099
Data scaling software	SCALA
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	48.246	2.300
High resolution limit [Å]	2.300	2.300
Number of reflections	22818	3244
<I/σ(I)>	16.1	1.4
Completeness [%]	100.0	100
Redundancy	70.2	71.6
CC(1/2)	1.000	0.900

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		294	3.5 M sodium formate 15% PEG 200 75 mM NaCl, 25 mM HEPES pH 7.9, 2.5 mM BME