6B7K
GH43 Endo-Arabinanase from Bacillus licheniformis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-11-20 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 64.558, 124.178, 69.231 |
Unit cell angles | 90.00, 91.16, 90.00 |
Refinement procedure
Resolution | 44.518 - 2.550 |
R-factor | 0.2317 |
Rwork | 0.230 |
R-free | 0.27350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1uv4 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.577 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.12rc1_2807) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.740 | 2.660 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.077 | 0.324 |
Rmeas | 0.108 | 0.457 |
Rpim | 0.076 | 0.322 |
Number of reflections | 27463 | 3271 |
<I/σ(I)> | 7.9 | 1.5 |
Completeness [%] | 77.3 | 75.6 |
Redundancy | 2.1 | 2 |
CC(1/2) | 0.979 | 0.756 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.05 | 291 | 0.1 mM HEPES pH 7.05, 10% PEG 4000 (w/v), 5% 2-propanol (v/v) |