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6B5M

Structure of PfCSP peptide 21 with human protective antibody CIS43

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 5.0.2
Synchrotron siteALS
Beamline5.0.2
Temperature [K]100
Detector technologyPIXEL
Collection date2016-09-28
DetectorDECTRIS PILATUS3 S 6M
Wavelength(s)1.0
Spacegroup nameC 1 2 1
Unit cell lengths93.477, 61.861, 75.055
Unit cell angles90.00, 105.51, 90.00
Refinement procedure
Resolution38.988 - 1.790
R-factor0.2082
Rwork0.207
R-free0.23470
RMSD bond length0.003
RMSD bond angle0.715
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwarePHENIX (1.10.1_2155)
Data quality characteristics
 Overall
Low resolution limit [Å]38.988
High resolution limit [Å]1.790
Number of reflections37099
<I/σ(I)>9.6
Completeness [%]94.7
Redundancy3.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP2930.1M Sodium Acetate Trihydrate pH 4.6, 2M Ammonium Sulfate

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