6B5M
Structure of PfCSP peptide 21 with human protective antibody CIS43
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 5.0.2 |
| Synchrotron site | ALS |
| Beamline | 5.0.2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-09-28 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 1.0 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 93.477, 61.861, 75.055 |
| Unit cell angles | 90.00, 105.51, 90.00 |
Refinement procedure
| Resolution | 38.988 - 1.790 |
| R-factor | 0.2082 |
| Rwork | 0.207 |
| R-free | 0.23470 |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.715 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 38.988 |
| High resolution limit [Å] | 1.790 |
| Number of reflections | 37099 |
| <I/σ(I)> | 9.6 |
| Completeness [%] | 94.7 |
| Redundancy | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1M Sodium Acetate Trihydrate pH 4.6, 2M Ammonium Sulfate |
