6B4G
Crystal structure of Chaetomium thermophilum Gle1 CTD-Nup42 GBM complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-12-11 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0332 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 84.482, 93.055, 229.669 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.864 - 2.648 |
R-factor | 0.2412 |
Rwork | 0.240 |
R-free | 0.27680 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.033 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_2006: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.900 | 2.730 |
High resolution limit [Å] | 2.648 | 2.650 |
Rpim | 0.026 | 0.450 |
Number of reflections | 53442 | 5142 |
<I/σ(I)> | 20.5 | 1.4 |
Completeness [%] | 99.8 | 97.6 |
Redundancy | 13.1 | 10.5 |
CC(1/2) | 1.000 | 0.669 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 294 | 0.1M MES pH 6.3, 12% (w/v) PEG 20,000 |