6B3I
Annexin A13a
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-G |
Synchrotron site | APS |
Beamline | 21-ID-G |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-06-12 |
Detector | MARRESEARCH |
Wavelength(s) | 0.9786 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 190.623, 93.815, 94.858 |
Unit cell angles | 90.00, 106.02, 90.00 |
Refinement procedure
Resolution | 39.909 - 2.600 |
R-factor | 0.1946 |
Rwork | 0.193 |
R-free | 0.22960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1w3w |
RMSD bond length | 0.002 |
RMSD bond angle | 0.348 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.600 |
Number of reflections | 49419 |
<I/σ(I)> | 11.7 |
Completeness [%] | 98.9 |
Redundancy | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 100 mM NaAcetate, 40 mM 1,2-butanediol, 0.8% PEG 8000 |