6B2T
Crystal structure of Xanthomonas campestris OleA H285D
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-30 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.968020 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 81.421, 84.996, 102.956 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.800 |
R-factor | 0.1759 |
Rwork | 0.172 |
R-free | 0.24690 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.011 |
RMSD bond angle | 1.555 |
Data reduction software | HKL-2000 (v705) |
Data scaling software | HKL-2000 (v705) |
Phasing software | REFMAC (5.8.0158) |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.850 |
High resolution limit [Å] | 2.800 | 7.590 | 2.800 |
Rmerge | 0.180 | 0.086 | 0.628 |
Rmeas | 0.196 | 0.095 | 0.684 |
Rpim | 0.076 | 0.038 | 0.267 |
Number of reflections | 18234 | 1024 | 887 |
<I/σ(I)> | 2.7 | ||
Completeness [%] | 100.0 | 100 | 99.7 |
Redundancy | 6.6 | 6 | 6.3 |
CC(1/2) | 0.991 | 0.869 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.2 | 292 | 16% PEG 8000, 105 mM potassium phosphate dibasic, 100 mM sodium citrate pH 4.2 |