6B28
Crystal structure of human STAC2 Tandem SH3 Domains Q347I (296-411)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 200 |
Detector technology | IMAGE PLATE |
Collection date | 2017-08-28 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54179 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 35.383, 49.707, 89.667 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.830 - 2.550 |
R-factor | 0.2233 |
Rwork | 0.222 |
R-free | 0.25170 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.535 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 44.830 | 35.000 | 2.630 |
High resolution limit [Å] | 2.550 | 5.830 | 2.550 |
Rmerge | 0.135 | 0.046 | 0.769 |
Rmeas | 0.158 | 0.055 | 0.915 |
Rpim | 0.082 | 0.030 | 0.489 |
Number of reflections | 5536 | 516 | 432 |
<I/σ(I)> | 6.5 | ||
Completeness [%] | 99.3 | 97.5 | 98.6 |
Redundancy | 3.4 | 3.2 | 3.1 |
CC(1/2) | 0.996 | 0.707 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.4 | 277.15 | 0.1M Bis-Tris, 0.2M lithium sulfate, 35% PEG3350 |