6AZH
Clostridium perfringens putative fatty acid metabolism regulator
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 23-ID-B |
| Synchrotron site | APS |
| Beamline | 23-ID-B |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2015-10-15 |
| Detector | MARMOSAIC 300 mm CCD |
| Wavelength(s) | 0.97935 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 39.869, 93.873, 55.067 |
| Unit cell angles | 90.00, 96.07, 90.00 |
Refinement procedure
| Resolution | 29.104 - 1.750 |
| R-factor | 0.1979 |
| Rwork | 0.196 |
| R-free | 0.22530 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.743 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | AutoSol |
| Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 29.104 |
| High resolution limit [Å] | 1.680 |
| Number of reflections | 39564 |
| <I/σ(I)> | 23.7 |
| Completeness [%] | 97.5 |
| Redundancy | 7.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 20% PEG 3350, 0.2 M Sodium Formate |
