6AZ6
Streptococcus agalactiae GntR
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 23-ID-B |
| Synchrotron site | APS |
| Beamline | 23-ID-B |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-10-16 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.97935 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 109.548, 105.172, 45.858 |
| Unit cell angles | 90.00, 112.44, 90.00 |
Refinement procedure
| Resolution | 27.843 - 1.909 |
| R-factor | 0.196 |
| Rwork | 0.194 |
| R-free | 0.22890 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.897 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 27.843 |
| High resolution limit [Å] | 1.909 |
| Number of reflections | 36686 |
| <I/σ(I)> | 16.29 |
| Completeness [%] | 98.5 |
| Redundancy | 4.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2 M tri-ammonium citrate, 12% PEG 3350 |
