6AYH

Salmonella enterica GusR

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 23-ID-D
Synchrotron site	APS
Beamline	23-ID-D
Temperature [K]	100
Detector technology	CCD
Collection date	2015-10-08
Detector	MARMOSAIC 300 mm CCD
Wavelength(s)	0.97939
Spacegroup name	P 21 21 2
Unit cell lengths	52.686, 55.230, 60.499
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	27.615 - 2.050
R-factor	0.1871
Rwork	0.183
R-free	0.22200
Structure solution method	SAD
RMSD bond length	0.003
RMSD bond angle	0.509
Phasing software	PHENIX
Refinement software	PHENIX (1.12_2829)

Data quality characteristics

	Overall
Low resolution limit [Å]	27.620
High resolution limit [Å]	2.050
Number of reflections	20844
<I/σ(I)>	10.3
Completeness [%]	99.1
Redundancy	5.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	298.15	25% PEG3350, 0.2M Ammonium Acetate, 0.1M Bis-Tris pH6.5