6AXN
F95C Epi-isozizaene synthase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL14-1 |
Synchrotron site | SSRL |
Beamline | BL14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-03-18 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 1.18 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 51.614, 46.787, 75.371 |
Unit cell angles | 90.00, 98.16, 90.00 |
Refinement procedure
Resolution | 32.530 - 1.900 |
R-factor | 0.159 |
Rwork | 0.157 |
R-free | 0.19060 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3kb9 |
RMSD bond length | 0.015 |
RMSD bond angle | 1.461 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (dev_1839) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 32.530 |
High resolution limit [Å] | 1.900 |
Number of reflections | 28111 |
<I/σ(I)> | 9.9 |
Completeness [%] | 98.8 |
Redundancy | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 294 | 0.2 M MgCl2.6H2O, 0.1 M bis-Tris (pH 6.5), 25% (w/v) PEG 3350 |