6AXK

Crystal structure of Fab311 complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 23-ID-B
Synchrotron site	APS
Beamline	23-ID-B
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-03-27
Detector	DECTRIS EIGER X 16M
Wavelength(s)	1.03320
Spacegroup name	P 21 21 21
Unit cell lengths	66.117, 44.729, 186.079
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.520 - 2.103
R-factor	0.2053
Rwork	0.204
R-free	0.23560
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	homology model
RMSD bond length	0.002
RMSD bond angle	0.663
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	PHASER
Refinement software	PHENIX ((1.11.1_2575: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	46.520	2.140
High resolution limit [Å]	2.100	2.100
Rpim	0.077	0.500
Number of reflections	32026
<I/σ(I)>	11
Completeness [%]	98.1
Redundancy	5.1
CC(1/2)	0.821	0.465

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		298	0.1M MES pH6.0 36% PEG400 5% PEG3000