6AW0
Crystal structure of CEACAM3 L44Q
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2017-07-14 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 92.810, 92.810, 155.940 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 79.750 - 2.430 |
R-factor | 0.2225 |
Rwork | 0.221 |
R-free | 0.24356 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qsq |
RMSD bond length | 0.007 |
RMSD bond angle | 1.333 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 79.750 | 2.620 |
High resolution limit [Å] | 2.430 | 2.430 |
Rmerge | 0.243 | 1.595 |
Rpim | 0.137 | 0.913 |
Number of reflections | 13227 | |
<I/σ(I)> | 8.2 | 1.2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.7 | 7.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 298 | 0.8M Ammonium Sulphate, 1% PEG 3350, 0.1M Bis Tris pH 5.5 |