6ATI
HLA-DRB1*1402 in complex with Vimentin-64Cit59-71
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-11-05 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | .95370 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 67.270, 76.870, 94.910 |
Unit cell angles | 90.00, 109.68, 90.00 |
Refinement procedure
Resolution | 33.629 - 1.980 |
R-factor | 0.192 |
Rwork | 0.190 |
R-free | 0.23330 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4mcy |
RMSD bond length | 0.004 |
RMSD bond angle | 0.885 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.629 | 2.090 |
High resolution limit [Å] | 1.980 | 1.980 |
Rpim | 0.056 | 0.195 |
Number of reflections | 63444 | 9163 |
<I/σ(I)> | 9.1 | 4.3 |
Completeness [%] | 99.9 | 99.3 |
Redundancy | 3.6 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.3 | 294 | 26% PEG 3350, 0.2M Potassium Nitrate, 0.1M Bis-Tris-Propane pH 7.3 |