6ASY
BiP-ATP2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4C |
Synchrotron site | NSLS |
Beamline | X4C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-02-08 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 |
Unit cell lengths | 75.829, 75.752, 78.791 |
Unit cell angles | 62.05, 62.23, 73.42 |
Refinement procedure
Resolution | 39.087 - 1.850 |
R-factor | 0.16 |
Rwork | 0.159 |
R-free | 0.18920 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.202 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELXD |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.850 |
Rmerge | 0.070 |
Number of reflections | 113887 |
<I/σ(I)> | 29.3 |
Completeness [%] | 97.8 |
Redundancy | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 18-22% PEG 1000, 0.1 M phosphate citrate (pH 4.2-7.0), and 0.2 M Li2SO4 |