6AO3
Crystal structure of the murine gasdermin D C-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-07-02 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.9800 |
Spacegroup name | P 1 |
Unit cell lengths | 45.300, 56.840, 81.840 |
Unit cell angles | 94.86, 102.79, 98.99 |
Refinement procedure
Resolution | 34.760 - 1.760 |
R-factor | 0.1625 |
Rwork | 0.161 |
R-free | 0.18570 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.016 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 79.200 | 1.810 |
High resolution limit [Å] | 1.760 | 1.760 |
Number of reflections | 75173 | 5506 |
<I/σ(I)> | 10.1 | 2.07 |
Completeness [%] | 97.1 | 95.8 |
Redundancy | 2.93 | 2.88 |
CC(1/2) | 0.995 | 0.555 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 295 | 25% (v/v) polyethylene glycol (PEG) 3350, 0.1 M Bis-Tris (pH 5.5), 0.2 M MgCl2 |