6AMJ
CAT192 Fab Wild Type
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-11-24 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.5419 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 55.950, 83.350, 104.910 |
Unit cell angles | 90.00, 104.77, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.713 | 2.620 |
High resolution limit [Å] | 2.490 | 2.490 |
Rmerge | 0.396 | |
Number of reflections | 32712 | 4715 |
<I/σ(I)> | 2.3 | |
Completeness [%] | 98.8 | |
Redundancy | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 12% PEG 8K, 0.1M Sodium cacodylate pH 6.0, 0.2M MgCl2 |