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6AMJ

CAT192 Fab Wild Type

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU FR-E+ SUPERBRIGHT
Temperature [K]100
Detector technologyCCD
Collection date2014-11-24
DetectorRIGAKU SATURN 944+
Wavelength(s)1.5419
Spacegroup nameP 1 21 1
Unit cell lengths55.950, 83.350, 104.910
Unit cell angles90.00, 104.77, 90.00
Refinement procedure
Resolution30.713 - 2.490
R-factor0.209
Rwork0.206
R-free0.26180
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4gsz 3skj
RMSD bond length0.003
RMSD bond angle0.473
Data reduction softwareiMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwarePHENIX (1.12_2829)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.7132.620
High resolution limit [Å]2.4902.490
Rmerge0.396
Number of reflections327124715
<I/σ(I)>2.3
Completeness [%]98.8
Redundancy2.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP27712% PEG 8K, 0.1M Sodium cacodylate pH 6.0, 0.2M MgCl2

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