6AKL
Crystal structure of Striatin3 in complex with SIKE1 Coiled-coil domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-11 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97853 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 39.282, 42.382, 91.228 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.048 - 1.750 |
R-factor | 0.1893 |
Rwork | 0.187 |
R-free | 0.21330 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6akk |
RMSD bond length | 0.007 |
RMSD bond angle | 0.774 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.780 |
High resolution limit [Å] | 1.750 | 1.750 |
Rmerge | 0.067 | |
Rmeas | 0.070 | |
Rpim | 0.020 | 0.376 |
Number of reflections | 16205 | 798 |
<I/σ(I)> | 28 | 2 |
Completeness [%] | 99.8 | 99.4 |
Redundancy | 12.5 | 11.4 |
CC(1/2) | 0.828 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 35% (v/v) MPD; 0.1 M imidazole pH 7.5 |