6AIX
Crystal structure of DXO in complex with adenosine 3', 5' bisphosphate and two magnesium ions
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-03-22 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.075 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 46.460, 87.872, 50.097 |
Unit cell angles | 90.00, 114.32, 90.00 |
Refinement procedure
Resolution | 40.512 - 1.800 |
R-factor | 0.1715 |
Rwork | 0.170 |
R-free | 0.19920 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.825 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 33976 | |
<I/σ(I)> | 21.7 | |
Completeness [%] | 98.9 | |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20% (w/v) PEG 3350, 100mM pAp, 10mM MgCl2 |