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6AHG

Trimeric structure of concanavalin A from Canavalia ensiformis

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron sitePAL/PLS
Beamline7A (6B, 6C1)
Temperature [K]100
Detector technologyCCD
Collection date2017-06-19
DetectorADSC QUANTUM 270
Wavelength(s)1.000
Spacegroup nameI 4 2 2
Unit cell lengths136.461, 136.461, 193.146
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution48.290 - 2.830
R-factor0.24502
Rwork0.243
R-free0.27919
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)5ygm
RMSD bond length0.009
RMSD bond angle1.636
Data reduction softwareXDS
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0073)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]48.2902.980
High resolution limit [Å]2.8302.830
Rmerge0.0980.457
Number of reflections222303172
<I/σ(I)>15.54.8
Completeness [%]99.8
Redundancy7.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP293Polyethylene glycol 400, 0.1 M Cadmium chloride hydrate, 0.1 M Sodium acetate trihydrate pH 4.6

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