6AF0
Structure of Ctr9, Paf1 and Cdc73 ternary complex from Myceliophthora thermophila
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 77 |
Detector technology | PIXEL |
Collection date | 2018-07-07 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9789 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 99.867, 237.789, 62.737 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 118.890 - 2.880 |
R-factor | 0.24829 |
Rwork | 0.245 |
R-free | 0.30929 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.362 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 118.890 | 2.950 |
High resolution limit [Å] | 2.880 | 2.900 |
Rmerge | 0.075 | 1.230 |
Number of reflections | 34480 | 1718 |
<I/σ(I)> | 24.7 | 1.4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 10.4 | 10.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2M potassium phosphate dibasic, 20% PEG 3350 |