6ACN
STRUCTURE OF ACTIVATED ACONITASE. FORMATION OF THE (4FE-4S) CLUSTER IN THE CRYSTAL
Experimental procedure
Spacegroup name | P 21 21 2 |
Unit cell lengths | 173.600, 72.000, 72.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 5.000 - 2.500 |
Rwork | 0.187 |
RMSD bond length | 0.017 |
RMSD bond angle | 3.500 |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 2.600 * |
High resolution limit [Å] | 2.500 * |
Rmerge | 0.134 * |
Total number of observations | 283187 * |
Number of reflections | 28269 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | ammonium sulfate | 3.7 (M) | |
2 | 1 | drop | Tris-HCl | 0.5 (M) | |
3 | 1 | reservoir | ammonium sulfate | 2.2 (M) | |
4 | 1 | reservoir | Tris-HCl | 0.5 (M) |