6A9U

Crystal strcture of Icp55 from Saccharomyces cerevisiae bound to apstatin inhibitor

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (2.4 Å)

Cell axes148.089148.089124.989
Cell angles90.0090.0090.00
SpacegroupI 4 2 2
Resolution limits47.76 - 2.40
the highest resolution shell value2.486 - 2.400
R-factor0.2268
R-work0.22470
the highest resolution shell value0.283
R-free0.26590
the highest resolution shell value0.323
RMSD bond length0.004
RMSD bond angle0.600

Data Collection Statistics

Resolution limits47.76 - 2.40
the highest resolution shell value -
Number of reflections27387
Rmerge_l_obs0.093
the highest resolution shell value0.824
Completeness99.9
Redundancy7.2
the highest resolution shell value6.1

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1MICROBATCH7293

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*