6A6G
Crystal structure of thermostable FiSufS-SufU complex from thermophilic Fervidobacterium Islandicum AW-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 7A (6B, 6C1) |
Synchrotron site | PAL/PLS |
Beamline | 7A (6B, 6C1) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-10-10 |
Detector | ADSC QUANTUM 270 |
Wavelength(s) | 0.979133 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 75.265, 76.969, 192.520 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.616 - 2.490 |
R-factor | 0.14962 |
Rwork | 0.146 |
R-free | 0.21390 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6A6E and 6A6F |
RMSD bond length | 0.013 |
RMSD bond angle | 1.511 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0218) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.540 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.129 | 0.435 |
Number of reflections | 39603 | |
<I/σ(I)> | 7.46 | |
Completeness [%] | 99.0 | |
Redundancy | 8.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2M lithium nitrate, PEG 3350, 0.1M HEPES, pH 7.0 |