6A66
Placental protein 13/galectin-13 variant R53H with Tris
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-07-01 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.98 |
Spacegroup name | C 2 2 2 |
Unit cell lengths | 58.231, 92.060, 50.682 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.115 - 1.400 |
R-factor | 0.1848 |
Rwork | 0.184 |
R-free | 0.19490 |
Structure solution method | MOLECULAR REPLACEMENT |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.115 | 1.420 |
High resolution limit [Å] | 1.400 | 1.400 |
Number of reflections | 27115 | |
<I/σ(I)> | 12.1 | |
Completeness [%] | 99.7 | |
Redundancy | 6.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | PEG |