6A64
Placental protein 13/galectin-13 variant R53HR55NH57RD33G with Lactose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-12-23 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.977 |
Spacegroup name | C 2 2 2 |
Unit cell lengths | 57.351, 92.583, 50.307 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 18.910 - 1.630 |
R-factor | 0.174 |
Rwork | 0.170 |
R-free | 0.20660 |
Structure solution method | MOLECULAR REPLACEMENT |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 18.910 | 1.660 |
High resolution limit [Å] | 1.630 | 1.630 |
Number of reflections | 17066 | |
<I/σ(I)> | 22.5 | |
Completeness [%] | 99.9 | |
Redundancy | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | PEG |