6A62

Placental protein 13/galectin-13 variant R53HH57RD33G with Lactose

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-12-23
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.977
Spacegroup name	C 2 2 2
Unit cell lengths	57.361, 92.659, 50.341
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	18.918 - 2.030
R-factor	0.1686
Rwork	0.164
R-free	0.21460
Structure solution method	MOLECULAR REPLACEMENT
Refinement software	PHENIX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	18.920	2.090
High resolution limit [Å]	2.030	2.030
Number of reflections	8973
<I/σ(I)>	26.3
Completeness [%]	99.8
Redundancy	6.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG