6A2W
Crystal structure of fucoxanthin chlorophyll a/c complex from Phaeodactylum tricornutum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-09-22 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 47.749, 115.718, 141.261 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.983 - 1.800 |
Rwork | 0.175 |
R-free | 0.19680 |
Structure solution method | SAD |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | CRANK2 |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.983 | 1.860 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.025 | 0.755 |
Rmeas | 0.035 | 1.068 |
Rpim | 0.025 | 0.755 |
Number of reflections | 36704 | 1157 |
<I/σ(I)> | 11.55 | 0.95 |
Completeness [%] | 67.0 | 31.86 |
Redundancy | 2 | 2 |
CC(1/2) | 1.000 | 0.721 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 293 | PEG 1000, calcium chloride, n-octal-D-thioglucoside, 4-Morpholineethanesulfonic acid hydrate |