6A1Y

Charcot-Leyden crystal protein/Galectin-10 variant Y35A

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-11-11
Detector	PSI PILATUS 6M
Wavelength(s)	0.98
Spacegroup name	P 65 2 2
Unit cell lengths	48.569, 48.569, 260.684
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.504 - 1.630
R-factor	0.1797
Rwork	0.178
R-free	0.19880
Structure solution method	MOLECULAR REPLACEMENT
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.504	1.660
High resolution limit [Å]	1.630	1.630
Number of reflections	23709
<I/σ(I)>	18.5
Completeness [%]	99.0
Redundancy	18.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	Bistris