6A1V

Charcot-Leyden crystal protein/Galectin-10 variant E33Q

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-11-11
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.98
Spacegroup name	P 65 2 2
Unit cell lengths	48.967, 48.967, 259.759
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	19.631 - 1.984
R-factor	0.2018
Rwork	0.199
R-free	0.23200
Structure solution method	MOLECULAR REPLACEMENT
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.980	2.030
High resolution limit [Å]	1.980	1.980
Number of reflections	13899
<I/σ(I)>	8.8
Completeness [%]	99.9
Redundancy	3.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	Bistris