6A02
Salmonella Typhi YfdX in the F222 space group at 1.4 A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2016-03-24 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.000 |
Spacegroup name | F 2 2 2 |
Unit cell lengths | 88.831, 92.459, 95.487 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.045 - 1.400 |
R-factor | 0.1899 |
Rwork | 0.189 |
R-free | 0.21290 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3dza |
RMSD bond length | 0.005 |
RMSD bond angle | 0.713 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.420 |
High resolution limit [Å] | 1.400 | 1.400 |
Rpim | 0.029 | 0.113 |
Number of reflections | 38242 | 1853 |
<I/σ(I)> | 41.3 | |
Completeness [%] | 98.8 | |
Redundancy | 9.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 293 | 0.1 M sodium acetate (pH 4.6), 2.5 M sodium chloride, 12% PEG1500, 1.5% 2-methyl-2,4-pentanediol |