6ZVA
Crystal structure of My5
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-2 |
| Synchrotron site | ESRF |
| Beamline | ID23-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-04-30 |
| Detector | MARMOSAIC 225 mm CCD |
| Wavelength(s) | 0.8726 |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 97.820, 97.820, 111.690 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 46.630 - 2.680 |
| R-factor | 0.204 |
| Rwork | 0.199 |
| R-free | 0.25120 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1bpv |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | BALBES |
| Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.910 | 2.810 |
| High resolution limit [Å] | 2.680 | 2.680 |
| Rmerge | 0.093 | 0.453 |
| Number of reflections | 5931 | 782 |
| <I/σ(I)> | 12.9 | |
| Completeness [%] | 100.0 | |
| Redundancy | 5 | |
| CC(1/2) | 0.992 | 0.799 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 1.9M ammonium sulfate 0.3M trisodium citrate |
