6ZKW
Crystal structure of InhA:01 TCR in complex with HLA-E bound to InhA (53-61)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-26 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 71.140, 108.670, 119.940 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 59.970 | 2.300 |
High resolution limit [Å] | 2.260 | 2.260 |
Rmerge | 0.069 | 1.183 |
Rpim | 0.028 | 0.616 |
Number of reflections | 44167 | 2150 |
<I/σ(I)> | 14.3 | 1.1 |
Completeness [%] | 99.7 | 97.95 |
Redundancy | 6.8 | 4.3 |
CC(1/2) | 0.999 | 0.352 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293.15 | 0.1 M TRIS pH 8.5, 25 % (w/v) PEG 4000, 15 % Glycerol |